Optimization of dispersive liquid–liquid microextraction procedure for detecting chlorpyrifos in human urine samples
نویسندگان
چکیده
منابع مشابه
hydrochlorothiazide detection in urine samples by hplc-dad and experimental design dispersive l-l microextraction
hydrochlorothiazide (hct) is a diuretic agent which is shown to be effective in the treatment of hypertension. literature reports have demonstrated that urinary excretion data may be used to assess the bioavailability of various formulations containing this thiazide. also hct consumption by the athletes is one of the drugs which should be regulated by world anti-doping agency (wada), because of...
Optimization of a Dispersive Liquid-Liquid Microextration Method for Analysis of Chlorpyrifos in Urine Using the Chemometrics Method
Aims: The use of simple, low cost, high -efficiency extraction methods for sample preparation in the forensic toxicology has been considered. Nowadays, the chemometrics technique can be used to determine the influencing factors on the response to optimize extraction methods. The aim of this study was to design and optimize a dispersive liquid-liquid microextraction (DLLME) method for extraction...
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A very simple, rapid and sensitive dispersive liquid-liquid microextraction (DLLME) followed by gas chromatography and flame ionization detection (GC-FID) was developed for the determination of phenol and carvacrol in honey samples. A mixture of 100 µl dichloromethane (extraction solvent) and 0.5 ml acetonitrile (disperser solvent) was rapidly injected into sample solution. Thereby a cloudy sol...
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A new, sensitive and fast dispersive liquid-liquid microextraction (DLLME) coupled with micro-solid phase extraction (μ-SPE) was developed for determination of zearalenone (ZEN) in wheat samples. The DLLME was performed using acetonitrile/water (80:20 v/v) as the disperser solvent and 1-octanol as the extracting solvent. The acetonitrile/water (80:20 v/v) solvent was also used to extract ZEN f...
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ژورنال
عنوان ژورنال: Medical Journal of The Islamic Republic of Iran
سال: 2019
ISSN: 1016-1430,2251-6840
DOI: 10.47176/mjiri.33.71